101 lines
8.5 KiB
XML
101 lines
8.5 KiB
XML
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<mods:title id="3C4D67FAC26ABFC291DBAC2FCDD7C001">Iridoid glucosides in the genus Sutera (Scrophulariaceae) as chemotaxonomic markers in tribe Limoselleae</mods:title>
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<mods:name id="DB40C33467EE2883F2754E96BA88B275" type="personal">
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<mods:roleTerm id="6BF8897B688D54CF6200B9B6F05BFA3D">Author</mods:roleTerm>
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<mods:namePart id="A09E1696F3DBAB0350ADA1DEFCDD5187">Gousiadou, Chryssoula</mods:namePart>
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<mods:affiliation id="FE00B7E4D8919BA3272920F9394084E7">∗ & Department of Chemistry, The Technical University of Denmark, Build. 207, DK- 2800 Lyngby, Denmark</mods:affiliation>
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<mods:namePart id="B355DFB6F057174399F5ED076F26C01E">Kokubun, Tetsuo</mods:namePart>
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<mods:roleTerm id="191F874FFE6E1EF12355E9323216DBD2">Author</mods:roleTerm>
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<mods:namePart id="DFA3A040F0D4A9ADCA241C891DA37113">Albach, Dirk C.</mods:namePart>
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<mods:namePart id="8D8B93DFAEC14E3F675DB0E2F89126ED">Gotfredsen, Charlotte H.</mods:namePart>
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<mods:namePart id="F894D01B95B09F9E1CEF4D89EB9A5650">Jensen, Søren Rosendal</mods:namePart>
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<mods:title id="34D8050510CC8AEACA17AB92148DCDB6">Phytochemistry</mods:title>
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<mods:date id="6F2D7D001069D553423B9C056D082444">2019</mods:date>
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<mods:number id="F3ABF59DD88E83EEA74EF629F2BFBABA">2019-02-28</mods:number>
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<mods:number id="FD34C12AE2D2FB9ABC6F1D3FB16DC5F0">158</mods:number>
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<mods:start id="E549C92FA57DBA54D89190184B5BC06E">149</mods:start>
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<mods:classification id="3778B5BDC7E0CFD5ECADC24B42C69EAD">journal article</mods:classification>
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<mods:identifier id="43B607B53B316DB354472F4B84EE6358" type="DOI">10.1016/j.phytochem.2018.10.021</mods:identifier>
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<mods:identifier id="B3B211184C8322B907F9E384EBF2BCC6" type="ISSN">1873-3700</mods:identifier>
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<treatment id="03DB683CFFEEFFB7FFC1FAD3FF6BF9A7" ID-DOI="http://doi.org/10.5281/zenodo.10576583" ID-Zenodo-Dep="10576583" LSID="urn:lsid:plazi:treatment:03DB683CFFEEFFB7FFC1FAD3FF6BF9A7" httpUri="http://treatment.plazi.org/id/03DB683CFFEEFFB7FFC1FAD3FF6BF9A7" lastPageNumber="153" pageId="4" pageNumber="153">
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<subSubSection id="C3688AA1FFEEFFB7FFC1FAD3FE35FAA2" box="[100,424,1386,1405]" pageId="4" pageNumber="153" type="nomenclature">
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<paragraph id="8BCDD92AFFEEFFB7FFC1FAD3FE35FAA2" blockId="4.[100,424,1386,1405]" box="[100,424,1386,1405]" pageId="4" pageNumber="153">
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<heading id="D0856E46FFEEFFB7FFC1FAD3FE35FAA2" bold="true" box="[100,424,1386,1405]" fontSize="36" level="1" pageId="4" pageNumber="153" reason="1">
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<emphasis id="B9060538FFEEFFB7FFC1FAD3FE35FAA2" bold="true" box="[100,424,1386,1405]" italics="true" pageId="4" pageNumber="153">
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3.3.
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<taxonomicName id="4C72A2A9FFEEFFB7FF37FAD3FE35FAA2" ID-CoL="3WT6H" authority="(L. fil.) Hilliard" box="[146,424,1386,1405]" class="Magnoliopsida" family="Scrophulariaceae" genus="Lyperia" kingdom="Plantae" order="Lamiales" pageId="4" pageNumber="153" phylum="Tracheophyta" rank="species" species="antirrhinoides" subGenus="Sutera">Lyperia (Sutera) antirrhinoides</taxonomicName>
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</emphasis>
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</heading>
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</paragraph>
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</subSubSection>
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<subSubSection id="C3688AA1FFEEFFB7FF20FA1BFF6BF9A7" pageId="4" pageNumber="153" type="description">
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<paragraph id="8BCDD92AFFEEFFB7FF20FA1BFF6BF9A7" blockId="4.[100,771,1442,1656]" pageId="4" pageNumber="153">
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Frozen plants (
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<quantity id="4C8A74CFFFEEFFB7FEB5FA1BFED8FA6A" box="[272,325,1442,1461]" metricMagnitude="-1" metricUnit="kg" metricValue="1.0" pageId="4" pageNumber="153" unit="g" value="100.0">100 g</quantity>
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) were blended with EtOH (300 ml) filtered and taken to dryness, and partitioned between H
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<subScript id="17F6DB6FFFEEFFB7FDACFA7EFD8FFA0C" attach="both" box="[521,530,1479,1491]" fontSize="5" pageId="4" pageNumber="153">2</subScript>
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O and Et
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<subScript id="17F6DB6FFFEEFFB7FDC3FA7EFDF2FA0C" attach="both" box="[614,623,1479,1491]" fontSize="5" pageId="4" pageNumber="153">2</subScript>
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O. The aqueous phase was concentrated (
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<quantity id="4C8A74CFFFEEFFB7FEC6FA63FE0FFA32" box="[355,402,1498,1517]" metricMagnitude="-3" metricUnit="kg" metricValue="1.6" pageId="4" pageNumber="153" unit="g" value="1.6">1.6 g</quantity>
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) and subjected to C
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<subScript id="17F6DB6FFFEEFFB7FDC1FA5AFDEBFA30" attach="left" box="[612,630,1507,1519]" fontSize="5" pageId="4" pageNumber="153">18</subScript>
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reverse-phase chromatography (Lobar size C), eluting with MeOH–H
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<subScript id="17F6DB6FFFEEFFB7FD23FA46FD12F9D4" attach="both" box="[646,655,1535,1547]" fontSize="5" pageId="4" pageNumber="153">2</subScript>
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O mixtures. Aucubin (
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<emphasis id="B9060538FFEEFFB7FF66F9A8FF52F9FB" bold="true" box="[195,207,1553,1572]" pageId="4" pageNumber="153">2</emphasis>
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) and melittoside (
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<emphasis id="B9060538FFEEFFB7FE27F9A8FE13F9FB" bold="true" box="[386,398,1553,1572]" pageId="4" pageNumber="153">3</emphasis>
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) was eluted with 25:1 while 8-
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<emphasis id="B9060538FFEEFFB7FD1AF9A8FD48F9FB" bold="true" box="[703,725,1553,1572]" italics="true" pageId="4" pageNumber="153">O-</emphasis>
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acetylharpagide (
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<emphasis id="B9060538FFEEFFB7FF46F994FF72F99F" bold="true" box="[227,239,1581,1600]" pageId="4" pageNumber="153">4</emphasis>
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) was eluted with 3:1. Unfortunately the amounts of the isolated compounds were not recorded. NMR spectra of the compounds are given in SI.
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</paragraph>
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</subSubSection>
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</treatment>
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</document> |